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71.
Crystal Structures and Phase Behavior of Sulfadiazine and a Method for the Preparation of Aggregates with Good Performance 下载免费PDF全文
Songgu Wu Shichao Du Mingyang Chen Kangli Li Lina Jia Dejiang Zhang Estevao G. J. Macaringue Baohong Hou Junbo Gong 《化学工程与技术》2018,41(3):532-540
The solvate and the solvent‐free form of sulfadiazine (SD) were investigated. SD was found to exist in one solvent‐free form and the N‐methylpyrrolidone (NMP) solvate form. The NMP solvate was shown to be a channel‐type compound. The intrinsic properties of the solvents were used to evaluate the effects of solubility on the phase transformation of SD and the NMP solvate. The SD phase could transform to the NMP solvate by NMP‐mediated phase transformation, which was governed by crystallization of the NMP solvate. The crystalline NMP solvate could transform to the solvent‐free solid state through solid‐solid transformation upon heating or water penetration‐mediated phase transformation. The rate of this water penetration‐mediated phase transformation of the NMP solvate to SD was unusually fast. It can be used to obtain SD aggregates of well‐defined shape and good powder properties. 相似文献
72.
73.
Rock joints infilled with sediments can strongly influence the strength of rock mass. As infilled joints often exist under unsaturated condition, this study investigated the influence of matric suction of infill on the overall joint shear strength. A novel technique that allows direct measurement of matric suction of infill using high capacity tensiometers (HCTs) during direct shear of infilled joints under constant normal stiffness (CNS) is described. The CNS apparatus was modified to accommodate the HCT and the procedure is explained in detail. Joint specimens were simulated by gypsum plaster using three-dimensional (3D) printed surface moulds, and filled with kaolin and sand mixture prepared at different water contents. Shear behaviours of both planar infilled joints and rough joints having joint roughness coefficients (JRCs) of 8–10 and 18–20 with the ratios of infill thickness to asperity height (t/a) equal to 0.5 were investigated. Matric suction shows predominantly unimodal behaviour during shearing of both planar and rough joints, which is closely associated with the variation of unloading rate and volumetric changes of the infill material. As expected, two-peak behaviour was observed for the rough joints and both peaks increased with the increase of infill matric suction. The results suggest that the contribution of matric suction of infill on the joint peak normalised shear stress is relatively independent of the joint roughness. 相似文献
74.
以河北承德某铁品位为61.08%,TiO2品位为7.66%的钒钛磁铁精矿为研究对象,进行了钒钛磁铁精矿深度还原-磁选试验研究。考察了还原温度、还原时间、C/O摩尔比、CaCO3添加量对还原产物和分选指标的影响。在还原温度为1350℃、还原时间120min、C/O摩尔比2.5、CaCO3添加量为16%、磁选场强为85mT的条件下,可以得到全铁品位为87.19%、铁回收率为82.62%的磁性产品和TiO2品位18.76%、TiO2回收率为79.40%非磁性产品。由还原产物的金属化率与XRD分析得知,钛磁铁矿向铁氧化物、钛氧化物和金属铁的转化较难发生,适当增加CaCO3的用量,能促进钛磁铁矿向CaTiO3、铁氧化物和金属铁的转化。 相似文献
75.
源距与屏蔽体厚度是直接影响可控中子孔隙度测井仪器测量准确性的重要参数。源距不仅影响测井仪器的测量误差,还影响测井仪器对地层孔隙度的灵敏度。屏蔽体厚度是保障测井响应完全反映地层的重要参数。从灵敏度、屏蔽率以及误差3个方面确定可控中子孔隙度测井仪器的源距与屏蔽体厚度。研究结果表明:近探测器源距越小,测井仪器灵敏度越高;近远探测器的间距对测量误差的影响随间距的增大,先减小再增大;当屏蔽率在70%以上且屏蔽率随厚度的变化较为缓慢时的屏蔽体厚度可作为屏蔽体最低厚度。 相似文献
76.
本文主要研究随机环境中配对依赖人口数两性 Galton-Watson 分枝过程的条件均值增长率的极限性质.利用上可加函数的性质,得到配对单元平均增长率的极限性质和该过程条件均值的上界和下界.文中给出了关于过程条件均值增长率的两个序列,利用配对单元平均增长率的性质,获得了这两个序列的极限性质.随机环境中配对依赖人口数两性分枝过程比较复杂,本文的结论推广了现有的研究成果. 相似文献
77.
Yadan Hou Shuhong Zhang Xuying Liu Jinzhou Chen Hui Li 《Color research and application》2020,45(4):699-709
Since smokers are becoming younger and younger, it is necessary to curb the tobacco epidemic at a younger age to prevent the devastating damage caused by tobacco products to future generations. This study focuses on the color schemes of cigarette packaging. It aims to find out color schemes of teenage consumers' disgust and apply them to cigarette packaging, which ultimately reduces the desire of purchasing and the smoking rate of young people. First, there were two ways to acquire color schemes. One was to extract the color schemes that can make teenagers disgust and keep them away from cigarette by association of psychological adjectives. The other way was to match achromatic colors with the chromatic colors that teenagers dislike in the questionnaire of 126 colors. Finally, eye movement experiment was used to verify the acquired color schemes meet the expected objectives of this study. A new idea to reduce the smoking rate of teenagers was proposed, and a method for the color design of cigarette packaging was provided. 相似文献
78.
为了使7075铝合金薄壁件表面喷丸加工应力得到松弛和均化,运用ANSYS建立平台式振动时效有限元模型,通过振动模态和谐响应分析,获得最佳激振频率和试样装夹位置。在此基础上,将薄壁框架件置于平台上进行振动时效处理,以验证仿真分析结果,评价其对试样表面应力作用效果。结果表明:在亚共振频率为112 Hz时,试样在平台零振幅和最大弯曲位置处分别对称布置,时效后表面均形成应力松弛,松弛率分别为29.5%和33.3%,不均匀波动分别为20.3%和20.7%,而沿振动方向松弛程度不均匀,说明激振力造成了材料表面组织屈服,且屈服程度与应力强度有关。提出再时效-位置交叠方法,使应力松弛不均匀度分别下降到9.9%和15.9%,应力均化得到改善,该研究工作为薄壁类零件表面应力均匀化提供了参考。 相似文献
79.
为了优化高碳马氏体不锈钢8Cr13MoV的球化热处理工艺,提高其退火后的冷加工性能,采用微观组织分析法以及拉伸力学分析法研究了球化退火过程中奥氏体化保温时间和冷却速率对8Cr13MoV钢的球化效果影响。结果表明, 随着奥氏体保温时间的增加,组织中细颗粒状碳化物数量减少,索氏体数量增多,试样硬度先降低后升高,但断后伸长率持续增加;随冷却速率增加,试样组织中细颗粒状碳化物和索氏体数量、硬度和强度增加,断后伸长率降低。综合对比,奥氏体保温时间ϕ90 min时试样综合力学性能较好,冷却速率应控制在25 ℃·h-1以内。与奥氏体保温时间相比,冷却速率对力学性能的影响更加显著。 相似文献
80.
The effect of biochar substituted for anthracite as reductant on magnetizing-roasting pyrite cinder was investigated.The key of magnetizing-roasting is the gasification reaction between reductants and CO2.Since biochar could react with CO2 more rapidly at lower temperature,the reactivity of biochar is better than that of anthracite.The gasification of biochar could produce reducing condition ofφCO/(φCO+φCO2)about 10%-20% between 700-800 ℃,which is in accord with the atmosphere and temperature of Fe2O3 reduction.So it is beneficial to the reduction of iron mineral of pyrite cinder.Compared with anthracite,biochar could decrease the roasting temperature from825 to 750 ℃ and roasting time from 20 to 15min,which shows that a better effect of magnetization could be obtained in the condition of lower temperature and shorter time.Using biochar as reductant,iron concentrate extracted from pyrite cinder as about 64%iron grade could be produced,and the recovery is over 90% under the condition of above 90% grinding particle less than 0.045 mm and magnetic intensity of 0.124-0.194 T. 相似文献